Which compound(s) in spearmint oil do you expect will be visible on the TLC plate under UV irradiation? Explain why. Compounds:R-carvone, R-limonene and (1R,2R,4R)-dihydrocarveol
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Which compound(s) in spearmint oil do you expect will be visible on the TLC plate under UV irradiation? Explain why.
Compounds:R-carvone, R-limonene and (1R,2R,4R)-dihydrocarveol
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- During TLC, what is the stationary phase and what is the mobile phase?Both melting points and TLC rely on differences in non covalent forces. Explain the role of these non-covalent interactions in the final answer obtained (melting point and Rf value).Higher Rf value will be obtained from dextrin than that of glucose in a reverse-phase TLC. True False
- Is ether a good solvent for TLC? What would be expected to be seen on a TLC plate if 2,6-dimethylaniline was spotted on lane 1 and 2,6-dimethylnitrobenzene on lane 2 and developed in ether?1. Which compound will have the largest Rf value on a TLC plate using 10% ethyl acetate/hexane as a developing solvent: 3- decanone or 3- decanol, toluene or benzoic acid, cyclohexane or cyclooctanone? Explain why?if you wanted to makes the spots travel up the TLC plate further, what solvent ration would you choose and why? 1:2 Ethyl acetate/Hexane, 2:3 Ethyl acetate/ Hexane, or 1:1 Ethyl acetate/Hexane
- So I completing a lab report and one of the sections is on TLC analysis. In the experiment, the TLC plate was submerged in toluene ethylacetate and had spots of cinnamon leaf oil, cinnamon aldehyde, and cinnamon bark oil. 9 spots total were seen under the UV light, but different spots appeared following a vanillin stain. Why is this so and what does this mean?Chemistry 1)Arrange the following in order of increasing Rf in TLC? 3-pentanone, 3-pentanol,pentane.2) If all your Rfs were too large, what would you do to your solvent system to bring themdown?• What solvent(s) would you try next?3) What would happen if you spotted too much compound on your TLC plate?4) One of the compounds we are examining today has a chiral center.• Which one has a chiral center?• Identify it.Arrange the following solvents in order of increasing polarity (least polar to most polar): Propyl Amine – Diethyl Ether – Ethyl Acetate- Octane If you ran an unknown sample on a TLC and observed only one spot with a Rf value of 0.95, is it safe to assume that it is a pure compound? If not, how can you check it out using TLC?
- The TLC plate shown was run in 80:20 Petroleum Ether - Ethyl acetate. If the eluent is changed to 95:5 Petroleum Ether - Ethyl Acetate, what will happen to the R-values? All Rf values will decrease All Rf values will increase Some Rf values will increase Some Rf values will decreaseHow would you discuss method of separation and identification of compounds in TLC?b. Answer the questions about the compounds below. جو عید بھید A OH B i) Which compound would have the highest Rf value by TLC? ii) Which compound would have the lowest Rf value by TLC? iii) Which compound would elute first in column chromatography? iv) Which compound would elute last in column chromatography?