Upon completing a synthesis, you attempt to purify your material via recrystallization. You dissolve the material in a minimal amount of hot solvent and then immediately place the vessel in an ice bath. You obtain the solid product through vacuum filtration. Any issues here? No issues, this is what you would do! O You may have an impure solid due to rapid cooling of the vessel. O You should have started with RT solvent to dissolve the material. O You should use gravity filtration for the fınal isolation.

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter80: Crystallization: Purification Of Solids
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Upon completing a synthesis, you attempt to purify your material via recrystallization. You dissolve
the material in a minimal amount of hot solvent and then immediately place the vessel in an ice
bath. You obtain the solid product through vacuum filtration. Any issues here?
No issues, this is what you would do!
You may have an impure solid due to rapid cooling of the vessel.
You should have started with RT solvent to dissolve the material.
You should use gravity filtration for the final isolation.
Transcribed Image Text:Upon completing a synthesis, you attempt to purify your material via recrystallization. You dissolve the material in a minimal amount of hot solvent and then immediately place the vessel in an ice bath. You obtain the solid product through vacuum filtration. Any issues here? No issues, this is what you would do! You may have an impure solid due to rapid cooling of the vessel. You should have started with RT solvent to dissolve the material. You should use gravity filtration for the final isolation.
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