The local anaesthetic lidocaine is required by the British Pharmacopoeia to contain not less than99.0% and not more than 101.0% of C14H22N2O, calculated with reference to the anhydroussubstance.0.2093 g of a lidocaine sample was dissolved in anhydrous acetic acid and titrated with 0.1025 Mperchloric acid. 8.53 mL was required. Another sample of the lidocaine from the same batch wasfound to contain 0.78% water. Does the sample meet the BP requirements?
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The local anaesthetic lidocaine is required by the British Pharmacopoeia to contain not less than
99.0% and not more than 101.0% of C14H22N2O, calculated with reference to the anhydrous
substance.
0.2093 g of a lidocaine sample was dissolved in anhydrous acetic acid and titrated with 0.1025 M
perchloric acid. 8.53 mL was required. Another sample of the lidocaine from the same batch was
found to contain 0.78% water. Does the sample meet the BP requirements?
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- A 4.912-g sample of a petroleum product was burnedin a tube furnace, and the SO2produced was collectedin 3% H2O2.Reaction:SO2(g)+H2O2→H2SO4A 25.00-mL portion of 0.00873 M NaOH was introducedinto the solution of H2SO4, following whichthe excess base was back-titrated with 15.17 mL of0.01102 M HCl. Calculate the sulfur concentrationin the sample in parts per million.the total solubility of amoxicillin hydrate a weekly acid acidic drug with a PK of 7.11 in SO 00.0 1M in acquiesce buffered solution of a pH equaling 7.2 isTitration of an oxalate sample gave the following percentages: 15.30 %, 15.59 % , and 15.57 % 1. Calculate the Average
- Caustic potash that has been exposed to air is found on analysis to contain 90.00% KOH, 2.38% K2CO3 and 7.62% H2O. What weight of residue will be obtained if 1.00 g of this sample is added to 46.00 mL of 1.00 N HCl and the resulting solution, after neutralization with 1.070N KOH is evaporated to dryness?A sample of alfalfa meal weighing 2.0 g is analyzed by Kjeldahl method for the percentage of nitrogen. The liberated NH3 is caught in a solution of H3BO3, and 8.23 ml of HCl are required in the subsequent titration. A sample of pure (NH4)2SO4 (132.12) weighing 0.61 g is treated with excess NaOH and the liberated NH3 (17.04) is also caught in H3BO3. The resulting solution requires 20 ml of the acid for titration. Calculate the percentage of protein in the sample using 6.25 as the factor.A 0.2985 g sample of an antibiotic powder was dissolved in HCl and the solution diluted to 100.0 mL. A 20.00 ml aliquot was transferred to a flask and followed by 25.00 ml of 0.01886 M KBRO3. An excess of KBr was added to form Br2, and the flask was stoppered. After 10 min, during which time the Br2 brominated the sulfanilamide, an excess of KI was added. The liberated iodine titrated with 12.88 ml of 0.1235 M sodium thiosulfate. Calculate the percent sulfanilamide (NH2C,H4SO2NH2) in the powder. Bro, + 5Br + 6H* 3Br, + 3H,0 NH2 NH2 Br. Br + 2B12 + 2H++ 2Br SO,NH2 SO,NH2 sulfanilamide Br, + 51 2Br + 12 excess 2 + 25,0,- 25,0,2 + 21- - MM: NH2C6H4SO2NH2 = 172.21 KBRO3 = 167.00 KBr 119.00
- A ferrous sulfate (BP) [FeSO4151.9g/mol] sample was analysed by titration using ammonium cerium (IV) nitrate (NH4)2Ce(NO3)6. The result shown 0.4980g of this sample used 25.50 ml 0.110M ammonium cerium (IV) nitrate. The BP specifies that ferrous sulfate material should contain not less than 86.0% and not more than 90.0% of FeSO4 Does the sample comply with the British Pharmacopoeia specification? A. The sample contains 85.6% ferrous sulfate thus does not comply with the British Pharmacopoeia specification B. The sample contains 85.6% ferrous sulfate thus complies with the British Pharmacopoeia specification C. The sample contains 86.0% ferrous sulfate thus complies with the British Pharmacopoeia specification D. The sample contains 89.0% ferrous sulfate thus complies with the British Pharmacopoeia specification E. The sample contains116.9% ferrous sulfate thus does not comply with the British Pharmacopoeia specification How do you work this out ?A 567.9 mg sample containing Na2CO3, NaHCO3 , NaOH and inert material was dissolved and titrated with 0.1002 M HCl. The titration required 24.30 mL to reach the phenolphthalein endpoint and an additional 38.67 mL to reach the methyl red endpoint. Determine the composition of the sample and the % of each titrated component.A 0.951-g sample containing (NH4)2C2O4 and compounds was dissolved in water and made alkaline with KOH. The liberated ammonia was distilled into 50.00 mL of 0.1007 N H2SO4. The excess H2SO4 was back titrated with 11.13 mL of 0.1214 N NaOH. Calculate the percentage of nitrogen in the sample.
- An alkaline sample of sodium compounds weighing 1.196 g was dissolved in water, cooled at 15 deg C, treated with 2 drops of phenolphthalein indicator and titrated with 1.058 N H2SO4 requiring 6.8 mL to render the solution colorless. Upon adding 2 drops of methyl orange and continuing the titration 16.5 mL more of the acid was needed to complete analysis. What is the quantitative composition of the sample?The concentration of ammonia in a cleaning product was determined by back titration.Firstly, 10.00 cm3 of the cleaning product was pipetted into a large conical flask,containing 250.00cm3 of 0.50 mol/l HCl to give Solution A.Following a period of reaction and shaking, 50.00cm3 of Solution A was removed anddiluted to 250 cm3 with water in a volumetric flask to give Solution B.20 cm3 samples of Solution B were titrated against 0.05 mol/l Na2CO3 solution, givingan average titre of 12.45 cm3. i) Write equations for the reactions that have taken place.ii) Determine the concentration of NH3 in the original cleaning product in mol/l,g/l, ppm, and % w/v.An antihistamine sample, brompheniramine maleate, weighing 5.01234 g was dissolved in alcohol and decomposed with metallic sodium. The resulting solution was treated with 12.00mL of 0.3121M AgNO3 to precipitate all of the liberated bromide ions as AgBr. The excess AgNO3 remaining in the solution was titrated with 9.123mL of 0.2181M KSCN to reach the endpoint. What is the %Br in the sample? Br- + Ag+ --> AgBr(s) Ag+ + SCN- --> AgSCN(s) Br = 79.904 g/mol