Properly annotate the NMR spectra of your unknown alcohol TFA ester. Make sure that you draw the structure of your parent alcohol on your spectra.

Chemistry for Today: General, Organic, and Biochemistry
9th Edition
ISBN:9781305960060
Author:Spencer L. Seager, Michael R. Slabaugh, Maren S. Hansen
Publisher:Spencer L. Seager, Michael R. Slabaugh, Maren S. Hansen
Chapter16: Amines And Amides
Section: Chapter Questions
Problem 16.27E
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Properly annotate the NMR spectra of your unknown alcohol TFA ester. Make sure that you draw the structure of your parent alcohol on your spectra.
Convert to
Picture
x X, AV v Aa v
SmartArt
Unknown Trifluoroacețate Esters
R-OH
R.
CF3
R
1-butyl
2-butyl (sec-butyl)
2-methyl-1-propyl (isobutyl)
1-pentyl
2-pentyl
3-pentyl
2-methyl-1-butyl
3-methyl-1-butyl (isoamyl)
1-hexyl
2-hexyl
cyclohexyl
benzyl
1-heptyl
1-octyl
2-оctyl
= Notes
Comments
ост
21
étv
MacBook Air
Transcribed Image Text:Convert to Picture x X, AV v Aa v SmartArt Unknown Trifluoroacețate Esters R-OH R. CF3 R 1-butyl 2-butyl (sec-butyl) 2-methyl-1-propyl (isobutyl) 1-pentyl 2-pentyl 3-pentyl 2-methyl-1-butyl 3-methyl-1-butyl (isoamyl) 1-hexyl 2-hexyl cyclohexyl benzyl 1-heptyl 1-octyl 2-оctyl = Notes Comments ост 21 étv MacBook Air
tfa3pro
tra3pro
H1 NMR- TFA Ester- Unk#3
tfa3pro
5.00
4.95
4.0
f1 (ppm)
1. (opm)
1.60
1.75
1.65
f1 (ppm)
5.2 5.0
4.8
4.6
4.4
4.2
4.0
1.2
1.0
0.8
0.6
0.4 0.2 0.0
2.8 2.6 2.4
f1 (ppm)
3.8
3.6
3.4
3.2
3.0
2.2 2.0
1.8
1.6
1.4
tfa#3
C13 NMR- TFA Ester- Unk#3
210 200 190
180
170
160 150
140 130
120
110
100
90
80
70
60
50
40
30
20
10
-10
-20
f1 (ppm)
Transcribed Image Text:tfa3pro tra3pro H1 NMR- TFA Ester- Unk#3 tfa3pro 5.00 4.95 4.0 f1 (ppm) 1. (opm) 1.60 1.75 1.65 f1 (ppm) 5.2 5.0 4.8 4.6 4.4 4.2 4.0 1.2 1.0 0.8 0.6 0.4 0.2 0.0 2.8 2.6 2.4 f1 (ppm) 3.8 3.6 3.4 3.2 3.0 2.2 2.0 1.8 1.6 1.4 tfa#3 C13 NMR- TFA Ester- Unk#3 210 200 190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 -10 -20 f1 (ppm)
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