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- Hexanoic acid was added to an immiscible biphasic solvent system, water and CCl4 at 20.0OC and the equilibrium concentrations of hexanoic acid were determined to be 3.66 g/L in H2O and 67.0 g/L in CCl4. Caluclate the distrubution coeffiecent (D2) of hexanoic acid in water with respect to CCl4.(b) Suppose the laboratory Technician carried out the same titration experiment in which he/she recorded an average volume of 20 cm³ of the dilute hydrochloric acid (HC) by titrating with 0.05 mol dm³ and 25 cm³ of potassium hydroxide (KOH). Calculate the concentration of hydrochloric acid from the Technician's experiment.Approximately 6.0mL of concentrated perchloric acid (70%) was transferred to a bottle and diluted with about 1.0L of water. A sample containing 251.5 mg of primary standard Na2B4O7.10H2O required 27.41 mL of the HClO4 solution to reach the methyl red end point. Calculate the molar concentration of the HClO4 (Fwt = 382g/mole)
- (b) The distribution ratio for X between n-hexane and water is 8.9. Calculate the concentration of X remaining in the aqueous phase after 50.0 mL of 0.200 M X is treated by extraction with the following quantities of n-hexane?Approximately 6 mL of concentrated perchloric acid (72%) was transferred to a bottle and diluted with about 1.0L of water. A sample containing 250.0 mg of primary standard sodium tetraborate (NazB407 .10H2O, FW= 381.42 g/mol) was dissolved in 50.00 mL water and required 27.25 mL of the HCIO4 solution to reach the methyl red end point. A 25.00 mL solution of an unknown NH3 sample required 13.24 mL of the HCIO4 solution. Calculate the molarity of the NH3.When a Vitamin C (ascorbic acid; MM = 176.12 g mol-1) tablet is crushed, dissolved and titrated with 0.0340 M KIO3(aq) to a purple/blue endpoint (given by a starch indicator), the volume of KIO3 used is 29.80 mL. If 60 mg of ascorbic acid is the recommended dietary allowance (i.e., 100% of the RDA), then what is the % RDA for the Vitamin C in the tablet? KIO3(aq) + 5 KI + 6 H+ → 3 I2(aq) + 3 H2O I2 (aq) + ascorbic acid → 2 I- + dehydroascorbic acid
- 1. (a) In the experiment carried out to determine the degree of association of benzoic acid in benzene (C6H6), the cooling curves of pure benzene and benzoic acid solution prepared by dissolving 0.358 g benzoic acid in 20 mL of benzene were obtained by using Beckmann thermometer, calibrated before the experiment. The cooling curves are given in the figure below. Calculate the degree of association of benzoic acid in benzene for the given solution. Ky= 5.055 K kg.mol-¹, dbenzene- 0.876 g.cm³, MBenzoic acid=122.12 g.mol-¹ T(°C) 2.88 2.38 Benzene Solution t(min)The solubility of suberic acid C6H12(COOH)2 is 0.14 g/100 ml H2O and 0.56g/100 ml ethyl ether at 15 0C. Calculate the weight of suberic acid removed from 50 ml aqueous solution containing 40 mg acid by extraction with 50 ml ether. Calculate the weight of acid that would be removed by two successive 25 ml extraction with ether.(A) if both sentences are true,(B) if both sentences are false,(C) if the first sentence is true but the second is false, and(D) if the first sentence is false but the second is true. 1. In the Winkler Titration Method, sodium thiosulfate is standardized against a known concentration of magnesium iodate. The normality (N) of a solution is always equal to its molarity (M). 2. In the experiment on determining the dissolved oxygen concentration of a water sample, the compound used to acidify the sample was hydrochloric acid. An acidic solution will have a pH greater than 7. 3. Radioactive wastes, like uranium, must be handled and disposed of according to special regulations designed to protect people and the environment. Nuclear power plants produce too much greenhouse gases due to the burning of uranium.
- A STOCK SOLUTION containing 0.1581 g/L K2CrO4 was prepared.In order to make the CALIBRATION STANDARD, 5 ml of the STOCK was transferredinto a 50ml volumetric flask and then diluted with an appropriate solvent.Calculate:(a) The ppm of K2CrO4 in the CALIBRATION STANDARD.(b) The molarity of K2CrO4 in the CALIBRATION STANDARD. (c) Calculate the molar absorptivity of K2CrO4 (at 371.0 nm). Assume that Beer's Law isobeyed over this concentration range.At 371.0 nm, this CALIBRATION STANDARD in a cell of path length 1.00 cm gave a %T of 59.752.A sample containing iron is approximately 99.0% w/w Fe. Using ammonia, iron is precipitated as Fe (OH)3 which is ignited to Fe203. (a) What is the gravimetric factor for analyte Fe (AW=55.85 g/mol) and precipitate Fe203 (FW=159.69 g/mol)? (b) What mass of sample is needed to ensure that the Fe203 precipitate would weigh at least 1.00 g?-3 . The densities of pure water and ethanol are 997 and 789 kg · m respectively. The partial molar volumes of water and ethanol are 17.8 × 10-³ and 55.2 × 10-³ L.mol-¹, respectively. Part A Calculate the change in volume relative to the pure components when 3.25 L of a solution with Tethanol = 0.524 is prepared. Express your answer to two significant figures and include the appropriate units. AV = 3.24 μà L ?