28 Report Sheet Separation of the Components of a Mixture D. Determination of Percent Recovery Mass of original sample 6.497 8 Mass of determined (NH4CI+ NaCl+ SiO2) 10.58 8 Differences in these weights 1-588 Percent recovery of matter g matter recovered .×100% = g original sample Account for your errors.

Fundamentals Of Analytical Chemistry
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Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.12QAP
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28 Report Sheet Separation of the Components of a Mixture
D. Determination of Percent Recovery
Mass of original sample
10.588
Mass of determined (NH Cl+ NaCl+ SiO2)
1-88 8
Differences in these weights
g matter recovered
Percent recovery of matter
%3D
= %00
%
g original sample
Account for your errors.
Combor
QUESTIONS
1. Could the separation in this experiment have been done in a different order? For example, if the mixture
was first extracted with water and then both the extract and the insoluble residue were heated to dryness,
could you determine the amounts of NaCl, NH,Cl, and SiO, originally present? Why or why not?
Consult a handbook to answer these questions.
2. How could you separate barium sulfate, BaSO4, from NaCl?
3. How could you separate magnesium chloride, MgCl2, from silver chloride, AgCl?
4. How could you separate tellurium dioxide, TeO2, from SiO,?
5. How could you separate lauric acid from a-naphthol? (See Table 3.1.)
Transcribed Image Text:28 Report Sheet Separation of the Components of a Mixture D. Determination of Percent Recovery Mass of original sample 10.588 Mass of determined (NH Cl+ NaCl+ SiO2) 1-88 8 Differences in these weights g matter recovered Percent recovery of matter %3D = %00 % g original sample Account for your errors. Combor QUESTIONS 1. Could the separation in this experiment have been done in a different order? For example, if the mixture was first extracted with water and then both the extract and the insoluble residue were heated to dryness, could you determine the amounts of NaCl, NH,Cl, and SiO, originally present? Why or why not? Consult a handbook to answer these questions. 2. How could you separate barium sulfate, BaSO4, from NaCl? 3. How could you separate magnesium chloride, MgCl2, from silver chloride, AgCl? 4. How could you separate tellurium dioxide, TeO2, from SiO,? 5. How could you separate lauric acid from a-naphthol? (See Table 3.1.)
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