Problem 131192089IR Spectrum(guid fim)68940003000200016001200800V (cm')100Mass Spectrum6380No significant UV60absorption above 220 nm4065M98/100/1028320C2H4CI24080120160200240280m/e13C NMR Spectrum(50.0 MHz. CDCI, solution)proton coupledsolventproton decoupled20016012080400 8 (ppm)H NMR Spectrum(200 MHz. CDCI, solution)expansions6.05.8 ppm22 2.0 ppmTMS5 43218 (ppm)108.6.102of base peak

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2089 IR Spectrum (liquid film) LL 4000 100 80 of base peak 3000 63 60 405 20 40 13C NMR Spectrum (50.0 MHz CDCI, solution) proton coupled www proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) 10 9 65 83 80 1 8 2000 V (cm¹) M** 98/100/102 120 160 m/e 160 my 689 1600 1200 200 120 800 Mass Spectrum C2H4Cl2 280 solvent 240 expansions 6.0 5.8 ppm J 7 6 5 1 J 80 2.2 2.0 ppm 4 Problem 13 No significant UV absorption above 220 nm 0 3 40 1 2 1 8 (ppm) TMS 1 119 0 8 (ppm)

2089 IR Spectrum (liquid film) LL 4000 100 80 of base peak 3000 63 60 405 20 40 13C NMR Spectrum (50.0 MHz CDCI, solution) proton coupled www proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) 10 9 65 83 80 1 8 2000 V (cm¹) M** 98/100/102 120 160 m/e 160 my 689 1600 1200 200 120 800 Mass Spectrum C2H4Cl2 280 solvent 240 expansions 6.0 5.8 ppm J 7 6 5 1 J 80 2.2 2.0 ppm 4 Problem 13 No significant UV absorption above 220 nm 0 3 40 1 2 1 8 (ppm) TMS 1 119 0 8 (ppm)

Organic Chemistry: A Guided Inquiry

2nd Edition

ISBN:9780618974122

Author:Andrei Straumanis

Publisher:Andrei Straumanis

ChapterL3: Carbon (13c) Nmr Spectroscopy

Section: Chapter Questions

Problem 9CTQ

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