Could I get some help with question 10, please? The first image includes the procedure. incesMailingsAa APA-FyestigateReview ViewE EMEYBiphenyl/Ethyl Acetate1= -ParagraphHelp2 T15FNo Spacing+ NaOH →Heading 1Ethyl AcetateNH3 CI10. How would your procedure change if you were to use dichloromethane as solvent instead of ethylacetate?GEStylesHCIlayıNA11. Now draw a flowchart to represent the experiment that was completed in lab. Include the molecularstructures for any cations and/or anions formed in the experiment. You can find a sample flowcharton Canvas under Module 4.4-Nitroaniline/ BiphenylAqогдHeading 2+Nack:FindRepliSeleEditin022-80 Page1IntroductionIn this experiment, you will be separating a mixture of 4-nitroaniline and biphenyl by extraction.Finally, you will identify and determine the purity of each compound. Usually, the extraction is usedas part of the 'work-up' after completing a chemical reaction. When part of a work-up, the productcould be isolated for other by-products of the reaction.1Experiment (Day 1)Dissolve about 1.0 g of the 4-nitroaniline /biphenyl (1:1 by mass) mixture in 10 mL of ethyl acetatein a 50 mL Erlenmeyer flask, and label this flask 1. Add 5 mL of 3 M aqueous hydrochloric acid (HCI)to the flask (note what happens), mix well, then pour off the mixture into a separatory funnel. Mixthe contents thoroughly by shaking vigorously for about 2-3 min with periodic venting (yourinstructor will demonstrate the correct technique for this). Allow the layers to separate completely,then drain off the lower layer into a second 50 mL Erlenmeyer flask (labeled flask 2). Add another 5mL of 3 M aqueous HCl solution to the separatory funnel, mix the contents as before, and drain offthe lower layer into flask 2. Exactly what chemical compound is present in flask 2?Drain off the upper layer into a 50 mL Erlenmeyer flask (see below, under "biphenyl"), and label this"flask 3". Return the contents of flask 2 into the separatory funnel, then add 2 mL of ethyl acetate andmix it thoroughly. Drain off the lower layer back into flask 2, then discard the upper ethyl acetatelayer into the designated waste. This is called backwashing and serves to remove any organicmaterial that might contaminate the contents of flask 2.lyof 3

The question is based on the concept of solvent extraction. we separate the components of the…

Answered: 10. How would your procedure change if…

Science

Chemistry

10. How would your procedure change if you were to use dichloromethane as solvent instead of ethyl acetate?

Organic Chemistry

8th Edition

ISBN:9781305580350

Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Chapter21: Benzene And The Concept Of Aromaticity

Section: Chapter Questions

Problem 21.63P

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You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.Your colleague is helping you develop the urine test. They suggest that the urine should be adjusted to a pH above 7 before extracting with the organic solvent. Why is this necessary? Support your explanation with a full arrow-pushing mechanism for the reaction that would occur if the pH was below 7. Include all formal charges, intermediates (if applicable) and products.
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You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.You find that methylphenidate is highly soluble in 2-methyltetrahydrofuran, a bio-renewable solvent. Draw the structure of 2-methyltetrahydrofuran and give two reasons why it is a good solvent choice for liquid-liquid extraction.
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Question 1 You are employed as a co-op student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated and the residue will be tested for the drug. You find that methylphenidate is highly soluble in 2-methyltetrahydrofuran, a bio-renewable solvent. Draw the structure of 2-methyltetrahydrofuran and give two reasons why it is a good solvent choice for liquid-liquid extraction. (Please find the image attached below to help you with this question) Question 2 (cont. from scenario 1). Your colleague is helping you develop the urine test. They suggest that the urine should be adjusted to a pH above 7 before…