1. You will be separating a binary mixture in this experiment. What are the two compounds in the binary mixture in this experiment? 2. The separation will be quite simple because one of the compounds is soluble in water and one is not. Which compound in the mixture is soluble and which is not? 3. From your reading of the experiment and the flow chart, come up with reasonable definitions or explanations of the terms residue and filtrate.

Appl Of Ms Excel In Analytical Chemistry
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Chapter3: Statistical Tests With Excel
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12:06 1
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38
Fundamental Chemistry I
39 of 116
Arkansas Scholastic Press
Purpose and Flow Chart for the Experiment
In this experiment, you will separate the components of a binary mixture of sand and
sodium chloride. You will collect data which will give you the information to calculate the
percentage of each component in the mixture and to calculate the percent of recovery for the
experiment.
The flow chart below summarizes the different steps you will take to complete the
experiment. This schematic represents the series of operations involved.
After drying and weighing the two components, you will calculate the percentage of each
component in the mixture. You will then calculate the percent recovery of the components in the
mixture.
Beaker #1
Sio, (s) + NaCl (s)
Add water and
perform gravity
filtration
Filtrate
NacI (aq)
Residue
SiO, (s)
Dry in Oven
@ 125° C
Evaporation to Dryness
on a Hot Plate
Cool to room temperature
and obtain mass of dry
filter paper and sand
Cool to room temperature
and obtain mass of dry
Naci
(g part)
(g whole)
% by mass =
х 100
% recovery = (g SiO, + g NaCl) x 100
(g original sample)
% error =L(g SiO, +NaCl - g original sample) | x 100
(g original sample)
Fundamental Chemistry I
39
Arkansas Scholastic Press
Transcribed Image Text:12:06 1 ull Done CHEM 1103 Lab Manual U... 38 Fundamental Chemistry I 39 of 116 Arkansas Scholastic Press Purpose and Flow Chart for the Experiment In this experiment, you will separate the components of a binary mixture of sand and sodium chloride. You will collect data which will give you the information to calculate the percentage of each component in the mixture and to calculate the percent of recovery for the experiment. The flow chart below summarizes the different steps you will take to complete the experiment. This schematic represents the series of operations involved. After drying and weighing the two components, you will calculate the percentage of each component in the mixture. You will then calculate the percent recovery of the components in the mixture. Beaker #1 Sio, (s) + NaCl (s) Add water and perform gravity filtration Filtrate NacI (aq) Residue SiO, (s) Dry in Oven @ 125° C Evaporation to Dryness on a Hot Plate Cool to room temperature and obtain mass of dry filter paper and sand Cool to room temperature and obtain mass of dry Naci (g part) (g whole) % by mass = х 100 % recovery = (g SiO, + g NaCl) x 100 (g original sample) % error =L(g SiO, +NaCl - g original sample) | x 100 (g original sample) Fundamental Chemistry I 39 Arkansas Scholastic Press
12:06 1
ull
Done CHEM 1103 Lab Manual U...
A student performed the experiment correctly and the initial massing correctly, but forgot to mass
the crucible cover after heating. What errors would this cause in the calculation of the percent of
water in the hydrate? Be specific.
36
Fundamental Chemistry I
Arkansas Scholastic Press
Lab 6. Separating the Components of a Binary Mixture
Lab 6 Pre-Lab
Name:
Date:
Instructor:
Time & Day of lecture:
1. You will be separating a binary mixture in this experiment. What are the two compounds in
the binary mixture in this experiment?
2. The separation will be quite simple because one of the compounds is soluble in water and one
is not. Which compound in the mixture is soluble and which is not?
3. From your reading of the experiment and the flow chart, come up with reasonable definitions
or explanations of the terms residue and filtrate.
4. A student was asked to determine the percentage of the components of a binary mixture
of KBr, potassium bromide, and Mg (OH),, magnesium hydroxide. The mass of the mixture
used was 6.321 grams. The student extracted the KBr with water since KBr is soluble in water
and Mg(OH), is not. The magnesium hydroxide remained in the container after the KBr was
extracted with water.
After evaporation of the filtrate, the KBr residue was dried and weighed. Its dry mass was
found to be 2.864g. The insoluble Mg(OH), was also dried and had a mass of 3.204 grams.
a. Calculate the percent of KBr in the mixture.
b. Calculate the percent of Mg(OH), in the mixture.
c. Calculate the percent of recovery using the total mass of substances recovered.
d. Calculate the percent error of this total recovery.
Fundamental Chemistry I
37
Arkansas Scholastic Press
Transcribed Image Text:12:06 1 ull Done CHEM 1103 Lab Manual U... A student performed the experiment correctly and the initial massing correctly, but forgot to mass the crucible cover after heating. What errors would this cause in the calculation of the percent of water in the hydrate? Be specific. 36 Fundamental Chemistry I Arkansas Scholastic Press Lab 6. Separating the Components of a Binary Mixture Lab 6 Pre-Lab Name: Date: Instructor: Time & Day of lecture: 1. You will be separating a binary mixture in this experiment. What are the two compounds in the binary mixture in this experiment? 2. The separation will be quite simple because one of the compounds is soluble in water and one is not. Which compound in the mixture is soluble and which is not? 3. From your reading of the experiment and the flow chart, come up with reasonable definitions or explanations of the terms residue and filtrate. 4. A student was asked to determine the percentage of the components of a binary mixture of KBr, potassium bromide, and Mg (OH),, magnesium hydroxide. The mass of the mixture used was 6.321 grams. The student extracted the KBr with water since KBr is soluble in water and Mg(OH), is not. The magnesium hydroxide remained in the container after the KBr was extracted with water. After evaporation of the filtrate, the KBr residue was dried and weighed. Its dry mass was found to be 2.864g. The insoluble Mg(OH), was also dried and had a mass of 3.204 grams. a. Calculate the percent of KBr in the mixture. b. Calculate the percent of Mg(OH), in the mixture. c. Calculate the percent of recovery using the total mass of substances recovered. d. Calculate the percent error of this total recovery. Fundamental Chemistry I 37 Arkansas Scholastic Press
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