PreLab D_ Chem 3AL_ Organic Chemistry Laboratory (Spring 2023)

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Monta Vista High *

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3AL

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Chemistry

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May 7, 2024

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pdf

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2/12/23, 9:55 PM PreLab D: Chem 3AL: Organic Chemistry Laboratory (Spring 2023) https://bcourses.berkeley.edu/courses/1521126/quizzes/2415110 1/8 * Some questions not yet graded PreLab D Due Feb 13 at 1pm Points 4 Questions 7 Available Feb 6 at 1pm - May 12 at 11:59pm Time Limit None Instructions Attempt History Attempt Time Score LATEST Attempt 1 213 minutes 3 out of 4 * Score for this quiz: 3 out of 4 * Submitted Feb 12 at 9:55pm This attempt took 213 minutes. Please read through Experiment 5 in the lab textbook, plus the procedural modifications on the Lab D Notebook Guide, before completing this assignment. Although the assignment is labeled a "quiz" by bCourses, there is no "timer" on your submission. You are welcome to consult with course materials, course staff, other students, and outside resources to help you understand the concepts addressed in the assignment, but copying-and-pasting-without-understanding (whether from other students or other sources) is strictly prohibited. Note: Only one attempt is permitted, so you should make sure not to actually click submit until you're satisfied with your final answers. Opening the assignment to see what the questions are, closing it, and then re-opening it later to continue working on it is fine! 0 / 0 pts Question 1 Are you submitting this assignment on time (prior to the start of your assigned lab section during the week of Feb 13-17)? If so, please write "YES" below. If not, please provide a short explanation.
2/12/23, 9:55 PM PreLab D: Chem 3AL: Organic Chemistry Laboratory (Spring 2023) https://bcourses.berkeley.edu/courses/1521126/quizzes/2415110 2/8 YES Correct! Correct! orrect Answers orrect Answers yes NA Yes. yes. n/a na YES. N/A Yes YES 0.6 / 0.6 pts Question 2 In Lab D Part 0, you will work with your teammates to choose an appropriate recrystallization solvent for adipic acid. Some possible recrystallization solvents are shown below. Look up the boiling points of each and fill in your answers below. SOLVENT NAME STRUCTURE BOILING POINT acetone [ Select ] ethanol 78 ºC diethyl ether [ Select ] hexane [ Select ] water 100 ºC Give one reason why diethyl ether isn't typically used as a recrystallization solvent: low boiling point means you'll lose all your solvent
2/12/23, 9:55 PM PreLab D: Chem 3AL: Organic Chemistry Laboratory (Spring 2023) https://bcourses.berkeley.edu/courses/1521126/quizzes/2415110 3/8 Answer 1: Answer 2: Answer 3: Answer 4: Answer 5: Answer 6: 56 ºC Correct! Correct! 78 ºC Correct! Correct! 35 ºC Correct! Correct! 69 ºC Correct! Correct! 100 ºC Correct! Correct! low boiling point means you'll lose all your solvent Correct! Correct! 0.6 / 0.6 pts Question 3 In Lab D Part I, you will start with 3 mL of room temperature (25 C) water. Based on the solubility data provided below, what are the maximum amounts of adipic and salicylic acid you can expect to dissolve in this much water at 25 C? Temp (°C) Solubility ( mg per 0.1 mL H O) Adipic Acid Salicylic Acid 100 >95 8.3 25 2.5 0.2 0 0.3 0.1 o o 2
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